Case Study

Cycle Development Using Freeze-Drying Microscopy (FDM) Differential Thermal Analysis (DTA) & Impedance Analysis

A customer approached BTL with a product that was being freeze-dried. Their current cycle duration was 64 hours, which they wanted to be reduced to increase throughput. FDM, DTA and impedance analysis was proposed to ascertain the lyophilisation and frozen state behaviour of the product, which could then be used to improve the cycle.

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